In today's fast-paced technology ecosystem, it is essential for students to stay updated with the latest advancements in instrumentation methods. This value added course can provide necessary skills and knowledge in this specific domain The primary objectives of this course are to provide hands-on training on sophisticated instruments, enabling participants to gain theoretical and practical experience. This can make participants familiarize with the principles, operations, data interpretation, and applications of various instruments. The students will learn how to use various sophisticated instruments such as UV-Visible, NMR, FTIR, SEM, TEM, GC-MS, XRD, HPLC TGA-DSC, Mass Spectroscopy. Faculty expertise from Chemistry Department, VIT Vellore will cover the topics and demonstration. Course outcomes are to enhance skills in operating sophisticated instruments. The course will also add to the employability of participants in various industries. Participants will also be equipped to pursue research as their career path.